The purpose of the study was to examine the relationship between selected motor fitness and volleyball playing ability for which 30 volleyball players were selected from Guru Ghasidas Vishwavidyalaya, Bilaspur (C.G.) and their age ranged from 18-28 years. The selected motor fitness: agility, coordination and reaction time test were measured by conducting side step test, eye-hand coordination (ball transfer) test and nelson finger reaction test. Brady’s volleyball skill test was used to assess the volleyball playing abilities of the selected subjects. Mean and Standard deviation were used as descriptive statistics. Pearson Product Moment Coefficient of correlation with significant level at 0.05 was used to examine the correlations between volleyball playing ability with agility, balance, coordination and reaction time. The statistical analysed was carried out using MS Excel and SPSS 16.0 version. The findings of the present study showed that there was significant relationship found in agility, coordination and reaction time in correlation between volleyball playing ability of Guru Ghasidas Vishwavidyalaya, Bilaspur (C.G.).